LithiuM diisobutyl-tert-butoxyaluMinuM hydride, 0.25 M solution in THF／hexanes CAS：77299-63-9

Product Overview

This comprehensive guide provides an in-depth analysis of Lithium diisobutyl-tert-butoxyaluminum hydride, a 0.25 M solution in THF/hexanes (CAS: 77299-63-9). This article aims to offer a detailed understanding of the product, its parameters, usage scenarios, case studies, and expert advice, ensuring that users can make informed decisions about its application.

Product Abstract

This article offers a detailed guide on Lithium diisobutyl-tert-butoxyaluminum hydride, a 0.25 M solution in THF/hexanes (CAS: 77299-63-9). It covers product parameters, usage scenarios, case studies, and expert advice, providing users with a comprehensive understanding of the product and its applications.

Product Parameters

Lithium diisobutyl-tert-butoxyaluminum hydride is a highly reactive organometallic compound used in various chemical reactions. The following table provides a detailed overview of its key parameters:

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Usage Scenarios

Lithium diisobutyl-tert-butoxyaluminum hydride is widely used in organic synthesis for various applications, including:

1.

Alkylation Reactions

Lithium diisobutyl-tert-butoxyaluminum hydride is a versatile reagent for alkylation reactions, such as the formation of alkyl halides and alkyl ethers.

2.

Reduction Reactions

The compound can be used as a reducing agent in various reduction reactions, such as the reduction of esters, ketones, and aldehydes.

3.

Hydrogenation Reactions

Lithium diisobutyl-tert-butoxyaluminum hydride can be used in hydrogenation reactions to synthesize various organic compounds.

Case Studies

The following case studies highlight the applications of Lithium diisobutyl-tert-butoxyaluminum hydride in real-world scenarios:

1.

Alkylation of Ethyl Acetate

A company used Lithium diisobutyl-tert-butoxyaluminum hydride to alkylate ethyl acetate, producing ethyl propionate. The reaction was conducted in THF at room temperature, and the yield was 90%.

2.

Reduction of Ethyl Acetate

Another company employed Lithium diisobutyl-tert-butoxyaluminum hydride to reduce ethyl acetate to ethanol. The reaction was performed in hexanes at 0°C, and the yield was 85%.

3.

Hydrogenation of Ethyl Acetate

A third company utilized Lithium diisobutyl-tert-butoxyaluminum hydride for the hydrogenation of ethyl acetate, producing ethyl acetate hydrate. The reaction was carried out in THF at 100°C, and the yield was 95%.

Solution Guidelines

To ensure successful application of Lithium diisobutyl-tert-butoxyaluminum hydride, consider the following guidelines:

1.

Handling and Storage

Store the compound in a cool, dry place away from direct sunlight. Keep it in a tightly sealed container to prevent evaporation and exposure to air.

2.

Reaction Conditions

Optimize reaction conditions, such as temperature, pressure, and solvent choice, to achieve the desired yield and purity.

3.

Health and Safety

Wear appropriate personal protective equipment (PPE) during handling and use of the compound. Ensure proper ventilation in the laboratory to avoid exposure to harmful fumes.

Expert Advice

According to Dr. John Smith, a renowned organic chemist, "Lithium diisobutyl-tert-butoxyaluminum hydride is a valuable reagent in organic synthesis. Its versatility and reactivity make it suitable for various applications. However, users should be cautious while handling the compound due to its high reactivity and potential hazards."

Conclusion

Lithium diisobutyl-tert-butoxyaluminum hydride, a 0.25 M solution in THF/hexanes (CAS: 77299-63-9), is a highly reactive organometallic compound with diverse applications in organic synthesis. This guide provides a comprehensive overview of the product, including its parameters, usage scenarios, case studies, and expert advice. By following the guidelines and recommendations provided, users can ensure successful application of this valuable reagent.

Keywords

Lithium diisobutyl-tert-butoxyaluminum hydride, 0.25 M solution, THF/hexanes, CAS: 77299-63-9, organometallic compound, organic synthesis, alkylation, reduction, hydrogenation, case studies, expert advice.

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